TA Instruments

AR1761-0001f

15/03/2013 16:42:47

Sample name	DI 40 mm AL P80
Sample notes	 
Experiment notes	DI Deionised water, 40 mm diameter. 70 mm total depth of water, 10 mm gap, with PE beads
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1761
Run number	1 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	15/03/2013 16:42:47

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	Yes
Initial temperature	20.0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:00:30 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 3.000 rad/s
End controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 300.0 rad/s
End controlled variable	velocity 3.000 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	20.0 C
Set temperature system idle	No

Geometry name	25mm ETC AL plate with studs
Geometry notes	Standard ETC AL parallel plate with studs
Geometry material	Aluminum
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	2.056 micro N.m.s^2
Geometry compliance	3.130E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	26500 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0.6 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.261 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	1
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	21.01 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Continuous ramp step 1

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0040	5.991	-49.441	10000	20.0	6.143	31.004	-16.12	7.489	-2.152	25030	5.3328	446.3	6.6660	666.60	3.411E-3	0.0	0.5
2.0040	9.802	13.265	10000	20.0	6.141	32.004	4.324	12.25	0.3529	25020	13.1535	166.7	16.442	1644.2	3.411E-3	0.0	0.5
3.0240	15.47	24.758	10000	20.0	6.144	33.024	8.070	19.34	0.4173	25030	26.8476	66.93	33.560	3356.0	3.411E-3	0.1	0.6
4.0080	18.42	32.626	10000	20.0	6.140	34.008	10.63	23.02	0.4620	25020	40.8083	47.21	51.010	5101.0	3.411E-3	0.1	0.6
5.0120	24.67	51.468	10000	20.0	6.141	35.012	16.78	30.84	0.5440	25020	67.9665	26.31	84.958	8495.8	3.411E-3	0.1	0.6
6.0040	31.56	76.369	10000	20.0	6.141	36.004	24.89	39.45	0.6309	25020	106.4450	16.07	133.06	13306	3.411E-3	0.1	0.6
7.0080	34.00	86.140	10000	20.0	6.138	37.008	28.08	42.50	0.6606	25010	126.2800	13.85	157.85	15785	3.411E-3	0.1	0.6
8.0120	39.28	107.88	10000	20.0	6.129	38.012	35.16	49.09	0.7163	24970	165.4180	10.36	206.77	20677	3.411E-3	0.1	0.6
9.0120	46.00	141.21	10000	20.0	6.130	39.012	46.03	57.51	0.8004	24980	222.9100	7.553	278.64	27864	3.411E-3	0.2	0.7
10.024	50.29	165.17	10000	20.0	6.125	40.024	53.84	62.86	0.8565	24960	268.4950	6.316	335.62	33562	3.411E-3	0.2	0.7
11.004	55.11	194.56	10000	20.0	6.115	41.004	63.42	68.89	0.9205	24920	319.4910	5.250	399.36	39936	3.411E-3	0.2	0.7
12.004	59.53	222.80	10000	20.0	6.109	42.004	72.62	74.41	0.9759	24890	370.7500	4.495	463.44	46344	3.411E-3	0.2	0.7
13.004	65.83	266.04	10000	20.0	6.103	43.004	86.71	82.28	1.054	24870	453.3720	3.673	566.72	56672	3.411E-3	0.2	0.7
14.008	70.47	300.32	10000	20.0	6.090	44.008	97.89	88.08	1.111	24810	517.1910	3.198	646.49	64649	3.411E-3	0.2	0.7
15.008	74.81	336.97	10000	20.0	6.089	45.008	109.8	93.51	1.175	24810	580.9240	2.837	726.16	72616	3.411E-3	0.3	0.8
16.004	78.91	371.48	10000	20.0	6.073	46.004	121.1	98.63	1.228	24740	684.7310	2.543	855.91	85591	3.411E-3	0.3	0.8
17.000	85.60	434.01	10000	20.0	6.062	47.000	141.5	107.0	1.322	24700	759.0980	2.157	948.87	94887	3.411E-3	0.3	0.8
18.012	89.90	472.87	10000	20.0	6.052	48.012	154.1	112.4	1.372	24660	835.4510	1.953	1044.3	1.0443E5	3.411E-3	0.3	0.8
19.004	94.00	512.42	10000	20.0	6.044	49.004	167.0	117.5	1.421	24630	912.2160	1.784	1140.3	1.1403E5	3.411E-3	0.3	0.8
20.020	100.6	580.95	10000	20.0	6.024	50.020	189.4	125.8	1.505	24540	1044.9500	1.551	1306.2	1.3062E5	3.411E-3	0.3	0.8
21.008	104.9	626.32	10000	20.0	6.006	51.008	204.1	131.1	1.557	24470	1134.3300	1.423	1417.9	1.4179E5	3.411E-3	0.4	0.9
22.004	109.0	676.22	10000	20.0	5.998	52.004	220.4	136.3	1.617	24440	1222.6100	1.316	1528.3	1.5283E5	3.411E-3	0.4	0.9
23.008	115.6	752.87	10000	20.0	5.966	53.008	245.4	144.5	1.699	24310	1375.1000	1.165	1718.9	1.7189E5	3.411E-3	0.4	0.9
24.004	119.8	801.49	10000	20.0	5.958	54.004	261.2	149.8	1.744	24280	1477.1600	1.082	1846.5	1.8465E5	3.411E-3	0.4	0.9
25.004	123.9	859.07	10000	20.0	5.939	55.004	280.0	154.9	1.807	24200	1578.0100	1.008	1972.5	1.9725E5	3.411E-3	0.4	0.9
26.004	130.2	938.88	10000	20.0	5.916	56.004	306.0	162.8	1.880	24100	1744.4900	0.9095	2180.6	2.1806E5	3.411E-3	0.4	0.9
27.004	134.5	997.06	10000	20.0	5.900	57.004	325.0	168.1	1.933	24040	1855.9900	0.8503	2320.0	2.3200E5	3.411E-3	0.5	1.0
28.004	140.6	1054.2	10000	20.0	5.870	58.004	343.6	175.8	1.954	23920	2028.8300	0.7738	2536.0	2.5360E5	3.411E-3	0.5	1.0
29.004	144.9	1151.5	10000	20.0	5.841	59.004	375.3	181.1	2.072	23800	2153.2300	0.7253	2691.5	2.6915E5	3.411E-3	0.5	1.0
30.012	149.2	1214.8	10000	20.0	5.822	60.012	396.0	186.5	2.123	23720	2280.5000	0.6822	2850.6	2.8506E5	3.411E-3	0.5	1.0
31.000	155.3	1303.1	10000	20.0	5.791	61.000	424.8	194.2	2.187	23590	2469.4500	0.6257	3086.8	3.0868E5	3.411E-3	0.5	1.0
32.004	159.4	1368.5	10000	20.0	5.766	62.004	446.1	199.3	2.238	23490	2602.2600	0.5915	3252.8	3.2528E5	3.411E-3	0.5	1.0
33.008	163.7	1445.4	10000	20.0	5.745	63.008	471.1	204.6	2.303	23410	2741.3000	0.5593	3426.6	3.4266E5	3.411E-3	0.6	1.1
34.004	169.9	1540.8	10000	20.0	5.701	64.004	502.2	212.3	2.365	23230	2950.7600	0.5152	3688.5	3.6885E5	3.411E-3	0.6	1.1
35.008	174.0	1620.8	10000	20.0	5.672	65.008	528.3	217.5	2.429	23110	3095.2700	0.4887	3869.1	3.8691E5	3.411E-3	0.6	1.1
36.000	178.2	1700.8	10000	20.0	5.663	66.000	554.4	222.8	2.488	23070	3247.9800	0.4649	4060.0	4.0600E5	3.411E-3	0.6	1.1
37.008	184.4	1815.8	10000	20.0	5.616	67.008	591.9	230.5	2.567	22880	3474.7100	0.4306	4343.4	4.3434E5	3.411E-3	0.6	1.1
38.008	188.4	1877.0	10000	20.0	5.589	68.008	611.8	235.6	2.597	22770	3625.8501	0.4104	4532.3	4.5323E5	3.411E-3	0.6	1.1
39.008	194.7	2005.4	10000	20.0	5.547	69.008	653.7	243.4	2.685	22600	3872.9600	0.3814	4841.2	4.8412E5	3.411E-3	0.7	1.2
40.004	198.9	2100.0	10000	20.0	5.529	70.004	684.5	248.6	2.754	22530	4036.3000	0.3646	5045.4	5.0454E5	3.411E-3	0.7	1.2
41.008	204.9	2204.4	10000	20.0	5.474	71.008	718.5	256.1	2.805	22300	4282.4800	0.3399	5353.1	5.3531E5	3.411E-3	0.7	1.2
42.008	209.0	2277.5	10000	20.0	5.446	72.008	742.3	261.3	2.841	22190	4460.9600	0.3249	5576.2	5.5762E5	3.411E-3	0.7	1.2
43.008	213.2	2370.2	10000	20.0	5.435	73.008	772.6	266.5	2.899	22140	4637.6299	0.3118	5797.0	5.7970E5	3.411E-3	0.7	1.2
44.004	219.3	2483.1	10000	20.0	5.378	74.004	809.4	274.1	2.953	21910	4901.0698	0.2916	6126.3	6.1263E5	3.411E-3	0.7	1.2
45.020	223.4	2563.2	10000	20.0	5.337	75.020	835.5	279.3	2.991	21740	5090.2798	0.2788	6362.9	6.3629E5	3.411E-3	0.8	1.3
46.028	229.6	2728.0	10000	20.0	5.291	76.028	889.2	287.0	3.098	21560	5375.2500	0.2617	6719.1	6.7191E5	3.411E-3	0.8	1.3
47.004	233.7	2817.2	10000	20.0	5.252	77.004	918.3	292.1	3.144	21400	5563.5298	0.2508	6954.4	6.9544E5	3.411E-3	0.8	1.3
48.004	237.7	2907.3	10000	20.0	5.228	78.004	947.6	297.1	3.189	21300	5760.5898	0.2413	7200.7	7.2007E5	3.411E-3	0.8	1.3
49.004	243.9	3051.4	10000	20.0	5.189	79.004	994.6	304.9	3.262	21140	6061.9502	0.2274	7577.4	7.5774E5	3.411E-3	0.8	1.3
50.008	248.0	3139.8	10000	20.0	5.147	80.008	1023	310.0	3.301	20970	6263.8398	0.2182	7829.8	7.8298E5	3.411E-3	0.8	1.3
51.012	254.0	3270.9	10000	20.0	5.057	81.012	1066	317.5	3.358	20600	6572.9302	0.2044	8216.2	8.2162E5	3.411E-3	0.9	1.4
52.004	258.2	3356.6	10000	20.0	5.017	82.004	1094	322.7	3.390	20440	6789.0098	0.1963	8486.3	8.4863E5	3.411E-3	0.9	1.4
53.004	264.3	3521.8	10000	20.0	4.992	83.004	1148	330.3	3.475	20340	7108.7700	0.1864	8886.0	8.8860E5	3.411E-3	0.9	1.4
54.000	268.3	3624.7	10000	20.0	4.938	84.000	1181	335.4	3.522	20120	7329.6699	0.1788	9162.1	9.1621E5	3.411E-3	0.9	1.4
55.004	272.5	3753.2	10000	20.0	4.896	85.004	1223	340.6	3.592	19950	7556.6001	0.1720	9445.8	9.4458E5	3.411E-3	0.9	1.4
56.004	278.6	3871.3	10000	20.0	4.845	86.004	1262	348.2	3.624	19740	7897.0801	0.1628	9871.4	9.8714E5	3.411E-3	0.9	1.4
57.004	282.6	4002.9	10000	20.0	4.805	87.004	1305	353.2	3.694	19580	8123.9800	0.1569	10155	1.0155E6	3.411E-3	1.0	1.5
58.008	288.8	4157.0	10000	20.0	4.715	88.008	1355	361.0	3.754	19210	8483.6602	0.1474	10605	1.0605E6	3.411E-3	1.0	1.5
59.020	292.8	4270.5	10000	20.0	4.683	89.020	1392	366.0	3.803	19080	8722.7305	0.1424	10903	1.0903E6	3.411E-3	1.0	1.5
60.004	298.8	4447.6	10000	20.0	4.643	90.004	1450	373.5	3.881	18920	9082.1201	0.1356	11353	1.1353E6	3.411E-3	1.0	1.5

Peak hold step

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

0.99600	300.0	4456.2	10000	20.0	4.587	91.996	1452	375.0	3.873	18690	270.0660	0.1329	337.58	33758	3.411E-3	0.0	1.5
1.9960	300.0	4482.6	10000	20.0	4.598	92.996	1461	375.0	3.896	18730	519.6690	0.1332	649.59	64959	3.411E-3	0.0	1.5
2.9960	300.0	4465.8	10000	20.0	4.630	93.996	1456	375.0	3.881	18860	896.5830	0.1341	1120.7	1.1207E5	3.411E-3	0.0	1.6
3.9960	300.0	4478.3	10000	20.0	4.633	94.996	1460	375.0	3.893	18880	1150.0000	0.1342	1437.5	1.4375E5	3.411E-3	0.1	1.6
4.9960	300.0	4482.9	10000	20.0	4.608	95.996	1461	375.0	3.897	18770	1399.2100	0.1335	1749.0	1.7490E5	3.411E-3	0.1	1.6
5.9920	300.0	4475.6	10000	20.0	4.624	96.992	1459	375.0	3.890	18840	1776.8500	0.1339	2221.1	2.2211E5	3.411E-3	0.1	1.6
7.0120	300.0	4463.3	10000	20.0	4.612	98.012	1455	375.0	3.879	18790	2027.4800	0.1336	2534.4	2.5344E5	3.411E-3	0.1	1.6
8.0000	300.0	4521.3	10000	20.0	4.613	99.000	1474	375.0	3.930	18790	2406.2400	0.1337	3007.8	3.0078E5	3.411E-3	0.1	1.7
9.0120	300.0	4493.1	10000	20.0	4.645	100.012	1465	375.0	3.906	18920	2673.4299	0.1346	3341.8	3.3418E5	3.411E-3	0.2	1.7
9.9960	300.0	4485.9	10000	20.0	4.614	100.996	1462	375.0	3.899	18800	2907.1499	0.1337	3633.9	3.6339E5	3.411E-3	0.2	1.7
10.996	300.0	4488.5	10000	20.0	4.574	101.996	1463	375.0	3.902	18640	3284.3101	0.1325	4105.4	4.1054E5	3.411E-3	0.2	1.7
12.012	300.0	4503.0	10000	20.0	4.664	103.012	1468	375.0	3.914	19000	3535.6299	0.1351	4419.5	4.4195E5	3.411E-3	0.2	1.7
13.004	300.0	4463.7	10000	20.0	4.600	104.004	1455	375.0	3.879	18740	3913.8701	0.1333	4892.3	4.8923E5	3.411E-3	0.2	1.7
14.012	300.0	4486.2	10000	20.0	4.639	105.012	1462	375.0	3.899	18900	4164.5801	0.1344	5205.7	5.2057E5	3.411E-3	0.2	1.8
15.008	300.0	4490.1	10000	20.0	4.610	106.008	1464	375.0	3.903	18780	4415.0898	0.1336	5518.9	5.5189E5	3.411E-3	0.3	1.8
16.012	300.0	4496.2	10000	20.0	4.659	107.012	1466	375.0	3.908	18980	4792.2002	0.1350	5990.3	5.9903E5	3.411E-3	0.3	1.8
16.996	300.0	4478.0	10000	20.0	4.584	107.996	1460	375.0	3.893	18680	5044.6099	0.1328	6305.8	6.3058E5	3.411E-3	0.3	1.8
17.996	300.0	4514.9	10000	20.0	4.656	108.996	1472	375.0	3.924	18970	5421.8198	0.1349	6777.3	6.7773E5	3.411E-3	0.3	1.8
18.996	300.0	4493.9	10000	20.0	4.606	109.996	1465	375.0	3.906	18770	5673.1001	0.1335	7091.4	7.0914E5	3.411E-3	0.3	1.8
20.000	300.0	4502.5	10000	20.0	4.682	111.000	1468	375.0	3.913	19080	5923.0898	0.1356	7403.9	7.4039E5	3.411E-3	0.3	1.9
20.996	300.0	4484.8	10000	20.0	4.584	111.996	1462	375.0	3.898	18680	6300.2900	0.1328	7875.4	7.8754E5	3.411E-3	0.3	1.9
21.996	300.0	4449.1	10000	20.0	4.570	112.996	1450	375.0	3.867	18620	6551.4800	0.1324	8189.4	8.1894E5	3.411E-3	0.4	1.9
22.996	300.0	4472.1	10000	20.0	4.634	113.996	1458	375.0	3.887	18880	6802.8301	0.1342	8503.5	8.5035E5	3.411E-3	0.4	1.9
24.000	300.0	4483.3	10000	20.0	4.603	115.000	1461	375.0	3.897	18750	7181.4502	0.1334	8976.8	8.9768E5	3.411E-3	0.4	1.9
25.236	300.0	4459.2	10000	20.0	4.608	116.236	1453	375.0	3.876	18770	7556.9600	0.1335	9446.2	9.4462E5	3.411E-3	0.4	1.9
25.996	300.0	4501.8	10000	20.0	4.635	116.996	1467	375.0	3.913	18880	7808.1299	0.1343	9760.2	9.7602E5	3.411E-3	0.4	1.9
26.996	300.0	4476.4	10000	20.0	4.635	117.996	1459	375.0	3.891	18890	8061.4600	0.1343	10077	1.0077E6	3.411E-3	0.4	2.0
27.996	300.0	4477.6	10000	20.0	4.598	118.996	1459	375.0	3.892	18730	8312.8398	0.1332	10391	1.0391E6	3.411E-3	0.5	2.0
28.996	300.0	4526.8	10000	20.0	4.651	119.996	1476	375.0	3.935	18950	8689.1699	0.1348	10861	1.0861E6	3.411E-3	0.5	2.0
30.032	300.0	4488.5	10000	20.0	4.668	121.032	1463	375.0	3.902	19020	8939.1504	0.1353	11174	1.1174E6	3.411E-3	0.5	2.0
30.996	300.0	4478.3	10000	20.0	4.616	121.996	1460	375.0	3.892	18810	9317.3799	0.1337	11647	1.1647E6	3.411E-3	0.5	2.0
31.996	300.0	4438.9	10000	20.0	4.538	122.996	1447	375.0	3.858	18490	9567.5498	0.1315	11959	1.1959E6	3.411E-3	0.5	2.0
32.996	300.0	4503.0	10000	20.0	4.680	123.996	1468	375.0	3.914	19070	9819.9902	0.1356	12275	1.2275E6	3.411E-3	0.5	2.1
33.992	299.9	4504.0	10000	20.0	4.618	124.992	1468	374.9	3.916	18820	10197.000	0.1339	12746	1.2746E6	3.411E-3	0.6	2.1
35.012	300.0	4477.4	10000	20.0	4.620	126.012	1459	375.0	3.892	18820	10447.000	0.1339	13059	1.3059E6	3.411E-3	0.6	2.1
35.996	300.0	4494.0	10000	20.0	4.647	126.996	1465	375.0	3.906	18930	10708.200	0.1346	13385	1.3385E6	3.411E-3	0.6	2.1
36.996	300.0	4481.5	10000	20.0	4.630	127.996	1461	375.0	3.895	18860	11075.300	0.1341	13844	1.3844E6	3.411E-3	0.6	2.1
37.996	300.0	4491.1	10000	20.0	4.633	128.996	1464	375.0	3.904	18870	11329.500	0.1342	14162	1.4162E6	3.411E-3	0.6	2.1
38.996	300.0	4470.8	10000	20.0	4.590	129.996	1457	375.0	3.886	18700	11704.800	0.1330	14631	1.4631E6	3.411E-3	0.6	2.2
39.996	300.0	4486.5	10000	20.0	4.623	130.996	1462	375.0	3.900	18840	11956.700	0.1340	14946	1.4946E6	3.411E-3	0.7	2.2
41.000	300.0	4467.9	10000	20.0	4.608	132.000	1456	375.0	3.883	18770	12206.200	0.1335	15258	1.5258E6	3.411E-3	0.7	2.2
41.996	300.0	4467.7	10000	20.0	4.615	132.996	1456	375.0	3.883	18800	12587.200	0.1337	15734	1.5734E6	3.411E-3	0.7	2.2
42.996	300.0	4482.4	10000	20.0	4.639	133.996	1461	375.0	3.896	18900	12834.800	0.1344	16044	1.6044E6	3.411E-3	0.7	2.2
44.012	300.0	4458.0	10000	20.0	4.584	135.012	1453	375.0	3.875	18680	13214.100	0.1328	16518	1.6518E6	3.411E-3	0.7	2.3
45.000	300.0	4490.1	10000	20.0	4.630	136.000	1464	375.0	3.903	18860	13463.200	0.1341	16829	1.6829E6	3.411E-3	0.8	2.3
46.000	300.0	4459.7	10000	20.0	4.632	137.000	1454	375.0	3.876	18870	13716.700	0.1342	17146	1.7146E6	3.411E-3	0.8	2.3
46.996	300.0	4478.0	10000	20.0	4.626	137.996	1460	375.0	3.892	18850	14094.800	0.1340	17619	1.7619E6	3.411E-3	0.8	2.3
48.020	300.0	4483.5	10000	20.0	4.637	139.020	1461	375.0	3.897	18890	14344.100	0.1344	17930	1.7930E6	3.411E-3	0.8	2.3
48.996	300.0	4453.4	10000	20.0	4.603	139.996	1452	375.0	3.871	18750	14596.600	0.1334	18246	1.8246E6	3.411E-3	0.8	2.3
49.996	300.0	4527.7	10000	20.0	4.658	140.996	1476	375.0	3.935	18980	14971.000	0.1349	18714	1.8714E6	3.411E-3	0.8	2.3
51.004	300.0	4485.8	10000	20.0	4.630	142.004	1462	375.0	3.899	18870	15222.300	0.1341	19028	1.9028E6	3.411E-3	0.9	2.4
52.004	300.0	4500.6	10000	20.0	4.660	143.004	1467	375.0	3.912	18990	15602.200	0.1350	19503	1.9503E6	3.411E-3	0.9	2.4
53.020	300.0	4499.4	10000	20.0	4.617	144.020	1467	375.0	3.911	18810	15850.700	0.1338	19813	1.9813E6	3.411E-3	0.9	2.4
54.012	300.0	4469.2	10000	20.0	4.586	145.012	1457	375.0	3.885	18680	16102.000	0.1329	20128	2.0128E6	3.411E-3	0.9	2.4
55.004	300.0	4480.3	10000	20.0	4.629	146.004	1460	375.0	3.894	18860	16480.301	0.1341	20600	2.0600E6	3.411E-3	0.9	2.4
56.012	300.0	4444.6	10000	20.0	4.607	147.012	1449	375.0	3.863	18770	16730.199	0.1335	20913	2.0913E6	3.411E-3	0.9	2.5
57.000	300.0	4509.2	10000	20.0	4.652	148.000	1470	375.0	3.920	18960	17116.400	0.1348	21396	2.1396E6	3.411E-3	1.0	2.5
58.004	300.0	4480.9	10000	20.0	4.639	149.004	1461	375.0	3.895	18900	17358.699	0.1344	21698	2.1698E6	3.411E-3	1.0	2.5
59.012	300.0	4471.0	10000	20.0	4.615	150.012	1457	375.0	3.886	18800	17611.400	0.1337	22014	2.2014E6	3.411E-3	1.0	2.5
60.068	300.0	4501.4	10000	20.0	4.594	151.068	1467	375.0	3.913	18720	17987.000	0.1331	22484	2.2484E6	3.411E-3	1.0	2.5

Continuous ramp step 2

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0040	296.2	4401.6	10000	20.0	4.697	153.004	1435	370.3	3.875	19140	309.6710	0.1396	387.09	38709	3.411E-3	0.0	2.6
2.0000	292.2	4243.4	10000	20.0	4.693	154.000	1383	365.3	3.786	19120	547.4310	0.1433	684.29	68429	3.411E-3	0.0	2.6
3.0120	286.1	4149.4	10000	20.0	4.769	155.012	1352	357.6	3.782	19430	905.7200	0.1520	1132.2	1.1322E5	3.411E-3	0.1	2.6
4.0120	281.9	3977.5	10000	20.0	4.778	156.012	1296	352.4	3.679	19470	1142.5100	0.1567	1428.1	1.4281E5	3.411E-3	0.1	2.6
4.9960	277.9	3885.2	10000	20.0	4.874	156.996	1266	347.4	3.646	19860	1367.8300	0.1646	1709.8	1.7098E5	3.411E-3	0.1	2.6
6.0040	271.8	3734.0	10000	20.0	4.936	158.004	1217	339.8	3.582	20110	1706.1200	0.1742	2132.7	2.1327E5	3.411E-3	0.1	2.6
6.9960	267.6	3620.8	10000	20.0	4.944	158.996	1180	334.6	3.528	20140	1934.8199	0.1799	2418.5	2.4185E5	3.411E-3	0.1	2.6
8.0120	261.7	3470.7	10000	20.0	5.014	160.012	1131	327.1	3.459	20430	2250.8501	0.1910	2813.6	2.8136E5	3.411E-3	0.1	2.7
9.0120	257.6	3374.7	10000	20.0	5.087	161.012	1100	322.0	3.416	20730	2466.5500	0.2000	3083.2	3.0832E5	3.411E-3	0.2	2.7
9.9960	253.4	3262.0	10000	20.0	5.074	161.996	1063	316.8	3.356	20670	2787.1001	0.2060	3483.9	3.4839E5	3.411E-3	0.2	2.7
11.004	247.4	3090.5	10000	20.0	5.091	163.004	1007	309.2	3.258	20740	2983.3000	0.2170	3729.1	3.7291E5	3.411E-3	0.2	2.7
12.012	243.3	3015.3	10000	20.0	5.195	164.012	982.8	304.1	3.232	21170	3183.5901	0.2289	3979.5	3.9795E5	3.411E-3	0.2	2.7
12.996	237.1	2859.1	10000	20.0	5.230	164.996	931.9	296.4	3.144	21310	3483.9399	0.2426	4354.9	4.3549E5	3.411E-3	0.2	2.7
13.996	233.0	2776.3	10000	20.0	5.260	165.996	904.9	291.2	3.108	21430	3678.7700	0.2527	4598.5	4.5985E5	3.411E-3	0.2	2.8
15.016	226.9	2663.8	10000	20.0	5.295	167.016	868.3	283.6	3.061	21580	3961.1299	0.2682	4951.4	4.9514E5	3.411E-3	0.3	2.8
15.996	222.8	2559.1	10000	20.0	5.309	167.996	834.1	278.4	2.996	21630	4147.1201	0.2790	5183.9	5.1839E5	3.411E-3	0.3	2.8
16.996	218.6	2462.1	10000	20.0	5.347	168.996	802.5	273.2	2.937	21780	4328.6299	0.2918	5410.8	5.4108E5	3.411E-3	0.3	2.8
17.996	212.6	2351.3	10000	20.0	5.414	169.996	766.4	265.7	2.884	22060	4591.3398	0.3124	5739.2	5.7392E5	3.411E-3	0.3	2.8
19.000	208.5	2259.5	10000	20.0	5.448	171.000	736.5	260.6	2.826	22200	4768.2402	0.3269	5960.3	5.9603E5	3.411E-3	0.3	2.9
20.016	202.2	2129.6	10000	20.0	5.482	172.016	694.1	252.8	2.746	22330	5024.4302	0.3496	6280.5	6.2805E5	3.411E-3	0.3	2.9
21.004	198.2	2050.0	10000	20.0	5.502	173.004	668.2	247.7	2.697	22420	5185.4702	0.3653	6481.8	6.4818E5	3.411E-3	0.4	2.9
21.996	194.1	1968.7	10000	20.0	5.521	173.996	641.7	242.6	2.645	22500	5348.0898	0.3822	6685.1	6.6851E5	3.411E-3	0.4	2.9
22.996	187.8	1843.4	10000	20.0	5.572	174.996	600.8	234.7	2.560	22700	5591.8398	0.4121	6989.8	6.9898E5	3.411E-3	0.4	2.9
24.012	183.7	1777.0	10000	20.0	5.619	176.012	579.2	229.6	2.523	22890	5742.5801	0.4344	7178.2	7.1782E5	3.411E-3	0.4	2.9
25.016	177.5	1663.1	10000	20.0	5.628	177.016	542.1	221.9	2.443	22930	5968.2998	0.4658	7460.4	7.4604E5	3.411E-3	0.4	3.0
26.012	173.3	1594.6	10000	20.0	5.667	178.012	519.8	216.6	2.400	23090	6117.5400	0.4921	7646.9	7.6469E5	3.411E-3	0.4	3.0
27.008	169.2	1513.9	10000	20.0	5.687	179.008	493.5	211.5	2.333	23170	6260.0498	0.5180	7825.1	7.8251E5	3.411E-3	0.5	3.0
27.996	163.1	1413.4	10000	20.0	5.736	179.996	460.7	203.8	2.260	23370	6460.4399	0.5625	8075.6	8.0756E5	3.411E-3	0.5	3.0
29.012	158.8	1354.8	10000	20.0	5.751	181.012	441.6	198.5	2.224	23430	6597.7598	0.5945	8247.2	8.2472E5	3.411E-3	0.5	3.0
30.000	152.6	1245.9	10000	20.0	5.780	182.000	406.1	190.7	2.129	23550	6791.4102	0.6475	8489.3	8.4893E5	3.411E-3	0.5	3.0
31.012	148.5	1194.2	10000	20.0	5.814	183.012	389.2	185.6	2.097	23690	6916.8901	0.6878	8646.1	8.6461E5	3.411E-3	0.5	3.1
32.048	144.3	1125.6	10000	20.0	5.841	184.048	366.9	180.3	2.035	23800	7041.1001	0.7319	8801.4	8.8014E5	3.411E-3	0.5	3.1
33.012	138.0	1030.7	10000	20.0	5.857	185.012	336.0	172.5	1.948	23870	7215.8799	0.8020	9019.9	9.0199E5	3.411E-3	0.6	3.1
34.012	133.9	969.49	10000	20.0	5.878	186.012	316.0	167.4	1.888	23950	7328.2798	0.8546	9160.4	9.1604E5	3.411E-3	0.6	3.1
35.164	127.5	886.36	10000	20.0	5.912	187.164	288.9	159.4	1.812	24090	7496.5698	0.9475	9370.7	9.3707E5	3.411E-3	0.6	3.1
35.996	123.2	829.39	10000	20.0	5.935	187.996	270.3	154.0	1.755	24180	7603.4502	1.019	9504.3	9.5043E5	3.411E-3	0.6	3.1
36.996	119.2	781.98	10000	20.0	5.943	188.996	254.9	148.9	1.711	24210	7703.2002	1.091	9629.0	9.6290E5	3.411E-3	0.6	3.1
37.996	114.9	726.92	10000	20.0	5.956	189.996	236.9	143.7	1.649	24270	7802.0098	1.175	9752.5	9.7525E5	3.411E-3	0.6	3.2
38.996	108.5	650.17	10000	20.0	5.979	190.996	211.9	135.6	1.563	24360	7945.2998	1.326	9931.6	9.9316E5	3.411E-3	0.6	3.2
39.996	104.4	597.73	10000	20.0	5.992	191.996	194.8	130.5	1.493	24410	8032.4302	1.434	10041	1.0041E6	3.411E-3	0.7	3.2
40.996	100.2	555.55	10000	20.0	6.001	192.996	181.1	125.2	1.446	24450	8119.5298	1.560	10149	1.0149E6	3.411E-3	0.7	3.2
42.012	93.48	494.04	10000	20.0	6.027	194.012	161.0	116.9	1.378	24560	8250.2500	1.798	10313	1.0313E6	3.411E-3	0.7	3.2
42.996	89.28	451.03	10000	20.0	6.035	194.996	147.0	111.6	1.317	24590	8325.1699	1.974	10406	1.0406E6	3.411E-3	0.7	3.2
44.016	85.05	407.90	10000	20.0	6.045	196.016	133.0	106.3	1.251	24630	8399.8799	2.179	10500	1.0500E6	3.411E-3	0.7	3.3
44.996	80.59	373.94	10000	20.0	6.051	196.996	121.9	100.7	1.210	24650	8473.6699	2.429	10592	1.0592E6	3.411E-3	0.7	3.3
46.012	74.04	313.82	10000	20.0	6.066	198.012	102.3	92.55	1.105	24710	8572.9297	2.885	10716	1.0716E6	3.411E-3	0.8	3.3
47.000	69.77	284.52	10000	20.0	6.076	199.000	92.74	87.22	1.063	24750	8635.1797	3.254	10794	1.0794E6	3.411E-3	0.8	3.3
48.012	65.23	251.36	10000	20.0	6.084	200.012	81.93	81.54	1.005	24790	8696.6797	3.728	10871	1.0871E6	3.411E-3	0.8	3.3
49.000	58.57	221.57	10000	20.0	6.100	201.000	72.22	73.21	0.9865	24850	8778.6797	4.637	10973	1.0973E6	3.411E-3	0.8	3.4
50.012	54.22	181.39	10000	20.0	6.102	202.012	59.12	67.78	0.8723	24860	8826.3301	5.411	11033	1.1033E6	3.411E-3	0.8	3.4
50.992	49.53	154.73	10000	20.0	6.106	202.992	50.44	61.91	0.8147	24880	8876.1201	6.491	11095	1.1095E6	3.411E-3	0.8	3.4
52.012	44.69	128.69	10000	20.0	6.110	204.012	41.95	55.87	0.7509	24890	8918.6201	7.976	11148	1.1148E6	3.411E-3	0.9	3.4
53.012	40.40	108.83	10000	20.0	6.116	205.012	35.47	50.50	0.7024	24920	8955.4102	9.770	11194	1.1194E6	3.411E-3	0.9	3.4
54.004	35.63	87.101	10000	20.0	6.118	206.004	28.39	44.54	0.6375	24930	8991.7900	12.57	11240	1.1240E6	3.411E-3	0.9	3.4
54.996	30.16	65.875	10000	20.0	6.123	206.996	21.47	37.69	0.5696	24950	9027.9004	17.56	11285	1.1285E6	3.411E-3	0.9	3.4
56.012	25.32	48.388	10000	20.0	6.125	208.012	15.77	31.65	0.4983	24960	9052.1299	24.91	11315	1.1315E6	3.411E-3	0.9	3.5
57.000	20.11	32.668	10000	20.0	6.131	209.000	10.65	25.14	0.4236	24980	9075.8096	39.54	11345	1.1345E6	3.411E-3	1.0	3.5
57.996	14.28	17.791	10000	20.0	6.132	209.996	5.799	17.86	0.3248	24980	9093.0898	78.36	11366	1.1366E6	3.411E-3	1.0	3.5
59.000	9.449	8.2383	10000	20.0	6.134	211.000	2.685	11.81	0.2273	24990	9104.4102	179.1	11381	1.1381E6	3.411E-3	1.0	3.5
59.996	6.015	2.9998	10000	20.0	6.137	211.996	0.9778	7.518	0.1301	25000	9109.1201	442.3	11386	1.1386E6	3.411E-3	1.0	3.5

